2-(3-BROMOPHENYL)-1,3-DIOXOLANE
- Name 2-(3-BROMOPHENYL)-1,3-DIOXOLANE
- CAS 17789-14-9
- Purity 99%
Product Details
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1.What is the 2-(3-BROMOPHENYL)-1,3-DIOXOLANE ?
2-(3-Bromophenyl)-1,3-dioxolane was used in the synthesis of acetal by arylation of 1-benzylpiperidin-4-amine.
-
-
3132-99-8
m-bromobenzoic aldehyde
-
-
107-21-1
ethylene glycol
-
-
17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide
| Conditions | Yield |
|---|---|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 5.5h;
Heating / reflux;
|
100%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 20 - 135 ℃;
|
98%
|
|
m-bromobenzoic aldehyde; ethylene glycol;
With
toluene-4-sulfonic acid;
In
toluene;
for 4h;
Heating / reflux;
With
sodium hydrogencarbonate;
In
water; toluene;
at 0 ℃;
|
97%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 130 ℃;
|
96%
|
|
With
molybdenum(VI) oxide on silica;
In
toluene;
at 110 ℃;
for 2.2h;
|
93%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 18h;
Reflux;
Dean-Stark;
Inert atmosphere;
|
88%
|
|
With
9.0 wt% H4[SiW12O40] on SiO2;
In
neat (no solvent);
at 60 ℃;
for 6h;
Reagent/catalyst;
chemoselective reaction;
|
81%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 45h;
Heating;
|
80%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 104h;
Heating;
|
68%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 140 ℃;
for 16h;
Dean-Stark;
Inert atmosphere;
|
65%
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 24h;
Heating;
|
|
|
With
toluene-4-sulfonic acid;
Inert atmosphere;
|
|
|
With
hydrogen; toluene-4-sulfonic acid;
In
toluene;
for 2h;
Temperature;
Time;
Reflux;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 135 ℃;
for 24h;
Dean-Stark;
Inert atmosphere;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 135 ℃;
for 15h;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 18h;
Dean-Stark;
Reflux;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
at 140 ℃;
for 16h;
Schlenk technique;
|
|
|
With
toluene-4-sulfonic acid;
In
toluene;
for 8h;
Reflux;
|
|
|
With
trichostatin A;
|
-
-
3132-99-8
m-bromobenzoic aldehyde
-
-
17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide
| Conditions | Yield |
|---|---|
|
With
toluene-4-sulfonic acid;
In
ethylene glycol; toluene;
|
100%
|
|
With
sodium hydroxide;
In
ethylene glycol; toluene;
|
99%
|
2.What is the CAS number for 2-(3-BROMOPHENYL)-1,3-DIOXOLANE ?
The CAS number of 2-(3-BROMOPHENYL)-1,3-DIOXOLANE is 17789-14-9.
More information of 2-(3-BROMOPHENYL)-1,3-DIOXOLANE 17789-14-9 are:
|
CAS?Number |
17789-14-9 |
|
Density |
1.515 g/cm3 |
|
Boiling Point |
278.509 °C at 760 mmHg |
|
Flash Point |
130.337 °C |
|
Vapor Pressure |
0.001mmHg at 25°C |
|
Refractive Index |
n20/D 1.563(lit.) |
|
HS CODE |
2932999099 |
|
PSA |
18.46000 |
|
LogP |
2.49450 |
3.What are another words for 2-(3-BROMOPHENYL)-1,3-DIOXOLANE ?
Synonyms?for?2-(3-BROMOPHENYL)-1,3-DIOXOLANE 17789-14-9:1,3-Dioxolane,2-(m-bromophenyl)- (8CI);2-(3-Bromophenyl)dioxolane;3-(1,3-Dioxolan-2-yl)phenyl bromide;3-Bromobenzaldehyde ethylene acetal;m-Bromobenzaldehyde ethylene acetal;
4.What is the molecular formula of 2-(3-BROMOPHENYL)-1,3-DIOXOLANE?
The chemical formula of ?2-(3-BROMOPHENYL)-1,3-DIOXOLANE is?C9H9BrO2 which containing 9 Carbon atoms,9 Hydrogen atoms,1 Bromine atoms and 2 Oxygen atoms,and the molecular weight of??2-(3-BROMOPHENYL)-1,3-DIOXOLANE?is 229.073.
5.What is 2-(3-BROMOPHENYL)-1,3-DIOXOLANE (17789-14-9) used for?
2-(3-BROMOPHENYL)-1,3-DIOXOLANE is an organic compound characterized by its unique structure, which features a bromophenyl group attached to a 1,3-dioxolane ring. 2-(3-BROMOPHENYL)-1,3-DIOXOLANE is known for its potential applications in various chemical and pharmaceutical processes due to its distinct chemical properties.
InChI:InChI=1/C10H11BrO2/c11-9-4-1-3-8(7-9)10-12-5-2-6-13-10/h1,3-4,7,10H,2,5-6H2
Relevant articles related to 2-(3-BROMOPHENYL)-1,3-DIOXOLANE:
|
Article |
Source |
|
SMALL MOLECULE DRUGS AND RELATED METHODS FOR TREATMENT OF DISEASES RELATED TO TDP-43, ALPHA-SYNUCLEIN, HUNTINGTIN'S PROTEIN AND TAU PROTEIN OLIGOMER FORMATION |
- Sheet 35, (2021/02/12) |
|
Ni-Catalyzed Reductive Cyanation of Aryl Halides and Phenol Derivatives via Transnitrilation |
Mills, L. Reginald,Graham, Joshua M.,Patel, Purvish,Rousseaux, Sophie A. L. supporting information, p. 19257 - 19262 (2019/12/02) |
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