Vat Brown 3
- Name Vat Brown 3
- CAS 131-92-0
- Purity 99%
Product Details
Top quality factory supply 131-92-0 Vat Brown 3 at low price
- Molecular Formula: C42H23N3O6
- Molecular Weight: 665.661
- Appearance/Colour: Odorless brown to dark brown powder.
- Melting Point: 180ºC
- Refractive Index: 1.831
- Boiling Point: 685.54°C (rough estimate)
- PSA: 142.27000
- Density: 1.537 g/cm3
- LogP: 7.52250
Vat Brown 3(Cas 131-92-0) Usage
|
Preparation |
N-(5-chloro-9,10-dioxo-9,10-dihydroanthracen-1-yl)benzamide and N-(4-amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)benzamide Condensation in the presence of copper, and then cyclized with sulfuric acid. |
|
Air & Water Reactions |
Insoluble in water. |
|
Reactivity Profile |
Vat Brown 3 is incompatible with oxidizing and reducing agents. . |
|
Fire Hazard |
Flash point data for Vat Brown 3 are not available. Vat Brown 3 is probably combustible. |
|
Flammability and Explosibility |
Notclassified |
|
Standard |
Ironing Fastness |
|
Fading |
Stain |
|
ISO |
5 |
|
AATCC |
5 |
|
General Description |
Odorless brown to dark brown powder. |
|
Properties and Applications |
brown. Deep red powder. Insoluble in water and Etanol, slightly soluble in Xylene for bordeaux red solution. In concentrated sulfuric acid for dark wine red, dilution to red light brown, flocks. Alkaline reduction leuco body for the color red; Acid reduction leuco for yellow brown. Is light brittle dye. To cotton affinity is poorer, less used in cotton dyeing. Suitable for direct printing, resist printing and aniline black color resist, also suitable for shallow, color of discharge. Suitable for cotton knits dyeing, more suitable for silk printing. But printing and dyeing fabric in sunlight exposure easy appear fiber brittle damage phenomenon. Can be used for viscose and wool dyeing, can also be processed into organic pigment. Standard Ironing Fastness Chlorine bleach Light Fastness Mercerized Oxygen bleach Soaping Fading Stain ISO 5 5 7 4-5 4-5 5 5 AATCC 5 5 7-8 4-5 4-5 |
InChI:InChI=1/C42H23N3O6/c46-37-24-14-7-8-15-25(24)38(47)34-33(37)30(44-42(51)22-12-5-2-6-13-22)20-28-23-18-19-27-32(35(23)45-36(28)34)40(49)26-16-9-17-29(31(26)39(27)48)43-41(50)21-10-3-1-4-11-21/h1-20,45H,(H,43,50)(H,44,51)
131-92-0 Relevant articles
PREPARATION METHOD OF ORIGINAL DYE OF VAT BROWN R
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Page/Page column 6, (2012/12/13)
A preparation method of original dye of ...
131-92-0 Process route
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-
128-89-2
4,5'-bis-benzoylamino-1,1'-imino-di-anthraquinone
-
-
131-92-0
4,9-bis-benzoylamino-16H -dinaphtho[2,3-a ;2',3'-i ]carbazole-5,10,15,17-tetraone
| Conditions | Yield |
|---|---|
|
With
sulfuric acid;
|
|
|
With
sodium chlorate; sulfuric acid;
In
water;
at 10 - 45 ℃;
Product distribution / selectivity;
|
|
|
With
aluminium trichloride; benzonitrile;
|
-
-
3571-23-1
N -(9,10-dioxo-9,10-dihydro-[1]anthryl)-benzamide
-
-
131-92-0
4,9-bis-benzoylamino-16H -dinaphtho[2,3-a ;2',3'-i ]carbazole-5,10,15,17-tetraone
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
3
steps
1.1: bromine; sodium chlorate / nitrobenzene
2.1: sodium carbonate / 1,2-dichloro-benzene / 0.5 h / 140 - 145 °C
2.2: 150 - 155 °C
2.3: 170 - 185 °C
3.1: sulfuric acid; sodium chlorate / water / 10 - 45 °C
With
sodium chlorate; sulfuric acid; bromine; sodium carbonate;
In
water; nitrobenzene; 1,2-dichloro-benzene;
|
131-92-0 Upstream products
-
128-89-2
4,5'-bis-benzoylamino-1,1'-imino-di-anthraquinone
-
3571-23-1
N -(9,10-dioxo-9,10-dihydro-[1]anthryl)-benzamide
-
82-45-1
1-amino-9,10-anthracenedione
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